{"id":11797,"date":"2015-08-18T22:33:20","date_gmt":"2015-08-19T04:33:20","guid":{"rendered":"https:\/\/www.tofwerk.com\/?p=11797"},"modified":"2020-07-13T11:57:38","modified_gmt":"2020-07-13T17:57:38","slug":"liutibaoyouwuicp","status":"publish","type":"post","link":"https:\/\/www.tofwerk.com\/ja\/icp-tof-fluid-inclusions\/","title":{"rendered":"\u6d41\u4f53\u5305\u6709\u7269\u306eICP-MS\u5206\u6790\u306b\u304a\u3051\u308bTOF\u306e\u5229\u70b9"},"content":{"rendered":"<p class=\"lead\">In a recent publication from ETH, Matthieu Harlaux and co-workers\u00a0compare the performance of quadrupole (Q), sector field (SF), and time-of-flight (TOF) based ICP-MS for the analysis of fluid inclusions in minerals.<\/p>\n<p><a href=\"http:\/\/pubs.rsc.org\/en\/Content\/ArticleLanding\/2015\/JA\/C5JA00111K#!divAbstract\" target=\"_blank\" rel=\"noopener noreferrer\">\u201cCapabilities of sequential and quasi-simultaneous LA-ICPMS for the multi-element analysis of small quantity of liquids (pl to nl): insights from fluid inclusion analysis&#8221;<\/a> \u00a0J. Anal. At. Spectrom., 2015<\/p>\n<p>Fluid inclusions were sampled with different laser ablation technologies, chosen based on the spectral acquisition rates of the mass analyzers. Due to their speed limitations, the scanning QMS and SFMS where coupled to commercial LA-cell technology with washout times of about 1 s. The TOFMS, which records all mass\/charge values simultaneously, was used with a small volume tube-type ablation cell having washout times as short as 30 ms.<\/p>\n<p style=\"text-align: left;\"><strong>ICP-TOFMS excelled\u00a0for the analysis of small fluid inclusions<\/strong><\/p>\n<ul>\n<li>ICP-TOF\u00a0recorded significantly more data points per inclusion and more isotopes of interest. Even the complex signal structure of multi-phase inclusions can be deciphered and related. e.g., to originate from aqueous phase or from halite, magnesium hydroxides, hematite or uranium crystallites respectively.<\/li>\n<li>ICP-TOFMS generally provided the best precision for all types of analyzed inclusions<\/li>\n<li>ICP-TOFMS demonstrated the best detection limits over the entire mass range for small inclusions of &lt;10 \u00b5m, especially for heavy elements with m\/Q &gt;85 Th.[\/fullwidth]<\/li>\n<\/ul>\n<p>On paper the sensitivity of ICP-TOFMS for single element analysis is similar to QMS-based instruments and lower than SF-ICP-MS. But TOF is the only mass analyzer that simultaneously measures\u00a0all mass\/charge values\u00a0and thus the only one which can be coupled to fast washout laser ablation equipment. Under \u2018real world\u2019 conditions with a reasonable set of measured isotopes and confronted with complex transient signals the TOFMS shows distinct advantages over the scanning instruments. The gain in S\/N through reduction of aerosol dispersion leads to improved precision and even lower detection limits compared to QMS and even SFMS setups.<\/p>\n","protected":false},"excerpt":{"rendered":"<p>\u201cCapabilities of sequential and quasi-simultaneous LA-ICPMS for the multi-element analysis of small quantity of liquids (pl to nl): insights from fluid inclusion analysis&#8221; \u00a0J. Anal. At. Spectrom., 2015 Fluid inclusions were sampled with different laser ablation technologies, chosen based on the spectral acquisition rates of the mass analyzers. Due to their speed limitations, the scanning QMS and SFMS where coupled to commercial LA-cell technology with washout times of about 1 s. The TOFMS, which records all mass\/charge values simultaneously, was used with a small volume tube-type ablation cell having washout times as short as 30 ms. ICP-TOFMS excelled\u00a0for the analysis of small fluid inclusions ICP-TOF\u00a0recorded significantly more data points per &#8230; <a title=\"\u6d41\u4f53\u5305\u6709\u7269\u306eICP-MS\u5206\u6790\u306b\u304a\u3051\u308bTOF\u306e\u5229\u70b9\" class=\"read-more\" href=\"https:\/\/www.tofwerk.com\/ja\/icp-tof-fluid-inclusions\/\" aria-label=\"The Advantages of TOF for ICP-MS Analysis of Fluid Inclusions \u306b\u3064\u3044\u3066\u3055\u3089\u306b\u8aad\u3080\">\u7d9a\u304d\u3092\u8aad\u3080<\/a><\/p>","protected":false},"author":4,"featured_media":13559,"comment_status":"closed","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":{"_acf_changed":false,"footnotes":""},"categories":[122],"tags":[],"product_notes":[103],"class_list":["post-11797","post","type-post","status-publish","format-standard","has-post-thumbnail","hentry","category-customer-research","product_notes-icptof"],"acf":[],"yoast_head":"<!-- This site is optimized with the Yoast SEO plugin v27.5 - https:\/\/yoast.com\/product\/yoast-seo-wordpress\/ -->\n<title>The Advantages of TOF for ICP-MS Analysis of Fluid Inclusions - TOFWERK<\/title>\n<meta name=\"robots\" content=\"index, follow, max-snippet:-1, max-image-preview:large, max-video-preview:-1\" \/>\n<link rel=\"canonical\" href=\"https:\/\/www.tofwerk.com\/ja\/liutibaoyouwuicp\/\" \/>\n<meta property=\"og:locale\" content=\"ja_JP\" \/>\n<meta property=\"og:type\" content=\"article\" \/>\n<meta property=\"og:title\" content=\"The Advantages of TOF for ICP-MS Analysis of Fluid Inclusions - TOFWERK\" \/>\n<meta property=\"og:description\" content=\"\u201cCapabilities of sequential and quasi-simultaneous LA-ICPMS for the multi-element analysis of small quantity of liquids (pl to nl): insights from fluid inclusion analysis&#8221; \u00a0J. Anal. At. Spectrom., 2015 Fluid inclusions were sampled with different laser ablation technologies, chosen based on the spectral acquisition rates of the mass analyzers. Due to their speed limitations, the scanning QMS and SFMS where coupled to commercial LA-cell technology with washout times of about 1 s. The TOFMS, which records all mass\/charge values simultaneously, was used with a small volume tube-type ablation cell having washout times as short as 30 ms. 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